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Novel magnetron sputtered ceramic YSiFe oxide as CMAS-resistant coatings for environmental barrier coatings.

Naraparaju, Ravisankar and Ott, Alexandra and Schulz, Uwe and Mechnich, Peter (2020) Novel magnetron sputtered ceramic YSiFe oxide as CMAS-resistant coatings for environmental barrier coatings. International Conference on Advanced Ceramics and Composites, 26-31, Daytona Beach, USA.

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Abstract

A novel YSiFe oxide coating has been developed and a suitable heat-treatment was applied to achieve the crystalline phases that are stable at high temperatures. The heat-treatment includes an isothermal heating at 1250 °C for 1h followed by a rapid cooling to room temperature. The resultant phases: X2-Yttria Mono Silicate (YMS), Yttrium Iron oxide and Yttria were found to be nano-crystalline in nature and were homogeneously distributed in the coating. The coating has been subjected to CMAS reaction by performing infiltration experiments at 1300 °C for different time intervals. It was found out that the studied YSiFe oxide coating has induced the both the intrinsic crystallisation of the CMAS melt and formed reaction products such as oxyapatite and garnet phases. The Fe diffusion from the YSiFe oxide coating into the glass reinforced the reactive crystallisation of CMAS leading to apatite and further garnet formation which consumed CMAS glass and prevented further infiltration. This novel coating has been proven to be a very good CMAS resistant coating and could therefore be a promising candidate for CMAS resistant multilayer EBCs.

Item URL in elib:https://elib.dlr.de/136005/
Document Type:Conference or Workshop Item (Speech)
Title:Novel magnetron sputtered ceramic YSiFe oxide as CMAS-resistant coatings for environmental barrier coatings.
Authors:
AuthorsInstitution or Email of AuthorsAuthor's ORCID iD
Naraparaju, RavisankarRavisankar.Naraparaju (at) dlr.deUNSPECIFIED
Ott, AlexandraUNSPECIFIEDUNSPECIFIED
Schulz, UweUwe.Schulz (at) dlr.dehttps://orcid.org/0000-0003-0362-8103
Mechnich, PeterPeter.Mechnich (at) dlr.deUNSPECIFIED
Date:January 2020
Refereed publication:Yes
Open Access:No
Gold Open Access:No
In SCOPUS:No
In ISI Web of Science:No
Status:Published
Keywords:Environmental barrier coatings, CMAS, apatite, garnet, YMS, YSiFe oxide
Event Title:International Conference on Advanced Ceramics and Composites
Event Location:Daytona Beach, USA
Event Type:international Conference
Event Dates:26-31
Organizer:American Ceramic Society
HGF - Research field:Aeronautics, Space and Transport
HGF - Program:Aeronautics
HGF - Program Themes:propulsion systems
DLR - Research area:Aeronautics
DLR - Program:L ER - Engine Research
DLR - Research theme (Project):L - Turbine Technologies (old)
Location: Köln-Porz
Institutes and Institutions:Institute of Materials Research > High Temperature and Functional Coatings
Institute of Materials Research > Structural and Functional ceramics
Deposited By: Naraparaju, Dr Ravisankar
Deposited On:19 Oct 2020 09:52
Last Modified:19 Oct 2020 09:52

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